IBM thermometer invention measures temps of nanoscale objects
The patent-pending invention has been described in the peer-review journal Nature Communications in a paper titled ‘Temperature mapping of operating nanoscale devices by scanning probe thermometry.’ The nanoscale measurement technique comes from the IBM lab which was previously responsible for inventing the scanning tunneling microscope and the atomic force microscope.
Accurately measuring the temperature of objects at the nanoscale has been challenging scientists for decades. Current techniques are not accurate and they typically generate artifacts, limiting their reliability.
In the 1980s, IBM scientists Gerd Binnig and the late Heinrich Rohrer wanted to directly explore a surface’s electronic structure and imperfections. The instrument they needed to take such measurements didn’t exist, yet. So they did what any good scientist would do: they invented one. It became known as the scanning tunneling microscope (STM), opening the door to nanotechnology. Just a few years later, the invention was recognized with the highest of hMore than 30 years later IBM scientists continue to follow in the footsteps of Binnig and Rohrer and with their latest invention.
“We started back in 2010 and simply never gave up. Previous research was focused on a nanoscale thermometer, but we should have been inventing a thermometer for the nanoscale—an important distinction. This adjustment led us to develop a technique which combines local thermal sensing with the measuring capability of a microscope—we call it scanning probe thermometry,” says Dr. Fabian Menges, an IBM postdoc and co-inventor of the technique.
The most common technique to measure temperature on the macroscale is to bring a thermometer into thermal contact with the sample. This is how a fever thermometer works. Once it’s placed under our tongue it equilibrates to our body temperature so that we can determine our temperature at a healthy 37ºC.
Unfortunately, it gets a little more challenging when using a thermometer to measure a nanoscopic object. For example, it would be impossible to use a typical thermometer to measure the temperature of an individual virus. The size of the virus is too small and the thermometer cannot equilibrate without sdisturbing the virus temperature.
To solve the challenge, IBM scientists developed a single scan non-equilibrium contact thermometry technique to measure the temperature of nanoscopic objects using a scanning probe. As the scanning probe thermometer and the object cannot thermally equilibrate at the nanoscale, two signals are measured simultaneously: a small heat flux, and its resistance to heat flow. Combining the two signal the temperature of nanoscopic objects can then be quantified for an accurate result.
“The technique is analogous to touching a hot plate and inferring its temperature from sensing the heat flux between our own body and the heat source. Essentially, the tip of the probe is our the hand. Our perception to hot and cold can be very helpful to get an idea of an objects temperature, but it can also be misleading if the resistance to heat flow is unknown,” explained IBM scientist Dr. Bernd Gotsmann and co-inventor.
Previously, scientists were not accurately including this resistance dependence; but only measuring the rate of the thermal energy transfer through the surface, know as heat flux. In the paper, the authors included the effects of local variations of thermal resistance to measure the temperature of an indium arsenide (InAs) nanowire, and a self-heated gold interconnect with a combination of a few-miliKelvin and few-nanometer spatial resolution.
“Not only is the scanning probe thermometer accurate, it meets the trifecta for tools: it’s easy to operate, simple to build, and very versatile, in that it can be used to measure the temperature of nano- and micro-sized hot spots that can locally effect the physical properties of materials or govern chemical reactions in devices such as transistors, memory cells, thermoelectric energy converters or plasmonic structures. The applications are endless,” says Menges.
The team began to see improvements in the development of the scanning probe thermometer 18 months ago when they moved their research into the new Noise Free Labs — six meters underground at the Binnig and Rohrer Nanotechnology Center on the campus of IBM Research-Zurich.
The environment, which shields the experiments from vibration, acoustic noise, electromagnetic signals and temperature fluctuations, helped the team achieve sub-milliKelvin precision.
“While we had the benefit of this unique room, the technique can also produce reliable results in normal environment,” says Menges.
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